Tan Guan Huat
University of Malaya, Malaysia
Title: Electrochemical preparation and characterization of gold nanoparticles graphite electrode: Application to myricetin antioxidant analysis
Biography
Biography: Tan Guan Huat
Abstract
Graphite has been an attractive material for electrochemical analysis due to it attributes in terms of its physical, chemical inertness and also because of its low cost, abundantly available, reusable and can be obtained in various forms such as rod, sheet, and flexible sheets. However its electrochemical properties are often a drawback when compared to other solid metal electrode, but this can be improved by surface modification of the graphite with noble metal nanoparticles. In recent years, antioxidant analysis by electrochemical techniques has been the focus of many studies; this is because the technique is sensitive, rapid and possible for field analysis. These advantages had overcome the problem of anti-oxidant analysis, which are sensitive to environment oxidation and therefore a fast analysis procedure is always preferable. In this present paper, we have carried out the electrochemical improvement of a recycled graphite electrode through an optimized procedure by electro-deposition of the gold nanoparticles on the graphite surface. An improvement on the electrochemical properties of the graphite by enhancement of its effective surface area, heterogeneous electron transfer rate, over potential and also the sensitivity has been observed. Application of the fabricated gold nanoparticles graphite electrode was also successfully optimized for the qualitative and quantitative analysis of myricetin.